Annealing parameters effect on microstructure evolution, tensile properties and deformation behaviors of direct-cold-rolled UNS S32101 duplex stainless steel with heterogeneous layered structure

Abstract

Microstructure evolution, strain-induced martensite transformation (SIMT) kinetics, tensile properties, deformation behaviors of UNS S32101 duplex stainless steel (DSS) with heterogeneous layered structure (HLS) were investigated. HLS composed of multiscale grains (spanning coarse, fine, and ultrafine grains) was prepared by direct cold rolling in combination with short-time annealing, being dominated by coarse-grained ferrite (CGed α) and fine-grained austenite (FGed γ). A quantitative SIMT kinetics model was established to predict the α′-martensite fraction at various strain/annealing parameters, indicating that increased average grain size (AGS) for γ not only contributed to the SIM formation but also promoted the monotonic increase of SIMT rate until annealing for 10 min. Relatively high stacking fault energy (SFE, 35.89∼39.34 mJ/m2) favored mechanical twinning as the dominant deformation mode of γ accompanied by SIMT and dislocation glide. And α deformation was mainly coordinated by wavy slip. Both SFE and Olson-Cohen parameters were strongly correlated with the γ AGS, which could reasonably interpret the dependence of SIMT on the AGS. The A and B values increased progressively with grain coarsening along with the rapid decline in SFE, facilitating the martensite formation. Further increasing the AGS beyond the peak region severely suppressed SIMT probably due to the low probability of martensite embryo generation at deformation twins (DTs) intersections, coinciding with the sharp decrease A value.