Anisotropy in creep properties and its microstructural origins of 12Cr oxide dispersion strengthened ferrite steels

Abstract

The anisotropy in creep properties and its microstructural origins in two oxide dispersion strengthened (ODS) steels (i.e., 12Cr-ODS-IMR and 12Cr-ODS-NIFS) were systematically investigated. Both ODS steels exhibited the anisotropic creep properties. The creep strength in longitudinal directions (LD) or extrusion directions (ED) specimens was better than that in transverse directions (TD) specimens. The microstructural characterizations revealed that both steels had elongated grains along the ED and relatively equiaxed grains in other orientations. Both steels had a streak-like distribution of precipitates along the ED that was composed of Ti-enriched precipitates and nano-scale oxide particles in local area. The fractography of the crept TD and LD specimens suggested that both steels fractured by the mixed ductile and brittle fracture modes. The propagation of cracks and intergranular decohesion along the boundaries of elongated grains were more severe in the TD specimens than in the LD specimens. The combined effects of elongated grain morphology with low grain shape aspect ratio and segregation of precipitates along the ED can explain the anisotropy in creep properties. The anisotropy in 12Cr-ODS-IMR steel was relatively higher than that in 12Cr-ODS-NIFS steel, and the additional cold rolling and lower final heat treatment temperature in 12Cr-ODS-IMR steel were responsible for it.