Abstract
The oxidation of hydroxylamine by bromine monochloride, by elementary chlorine in hydrochloric acid medium, and by bromate and bromic acid has been investigated. Oxidation by bromine monochloride is utilised for the analytical determination of hydroxylamine. Detailed examination of the reaction of bromate with hydrochloric acid proves that, in the presence of excess of hydrochloric acid, these compounds quickly react forming bromine monochloride and elementary chlorine. The proportions of the reaction products have been determined. On the basis of the results of these investigations, it is possible to present an interpretation of the analytical method suggested by Kurtenacker for the determination of hydroxylamine.
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