Year-end Sale % OFF 
Abstract
The analytical performance of a spark sampling device “Aspect” (“VMK-Optoelektronika”) is evaluated for steel analysis by atomic emission spectrometry with inductively coupled plasma (ICP-AES). The results of studying the effect of pulse duration, frequency and current of the spark discharge on the character of sample erosion, size and quantity of aerosol particles are presented. The dependences of the analytical signal on the spark duration are obtained and the optimal duration of preliminary sparking is specified. The limit of Cr, Cu, Mn, Mo, Ni, P, Si, and V detection ranges from n x 10 5 to n x 10 2 % wt. The accuracy of the ICP-AES analysis with a spark sampling using standard reference sample showed the good agreement between certified and determined values of analyte concentration.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
