Abstract

This studied aimed at improving the mechanical properties for a new biopolymer feedstock using laser-sintering technology, especially when its laser-sintered parts are intended to be applied in the industrial and medical fields. Process parameter optimization and thermal post-processing are two approaches proposed in this work to improve the mechanical properties of laser-sintered 10 wt % cellulose-polylactic acid (10%-CPLA) parts. Laser-sintering experiments using 23 full factorial design method were conducted to assess the effects of process parameters on parts’ mechanical properties. A simulation of laser-energy distribution was carried out using Matlab to evaluate the experimental results. The characterization of mechanical properties, crystallinity, microstructure, and porosity of laser-sintered 10%-CPLA parts after thermal post-processing of different annealing temperatures was performed to analyze the influence of thermal post-processing on part properties. Image analysis of fracture surfaces was used to obtain the porosity of laser-sintered 10%-CPLA parts. Results showed that the optimized process parameters for mechanical properties of laser-sintered 10%-CPLA parts were laser power 27 W, scan speed 1600 mm/s, and scan spacing 0.1 mm. Thermal post-processing at 110 °C produced best properties for laser-sintered 10%-CPLA parts.

Highlights

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  • The annealing temperature should be higher than the Tg of 10%-CPLA because the motion of molecular chains only starts above Tg

  • Thescheme laser energy, density, mechanical properties responding to the full factorial designof design are listed in and

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Summary

Introduction

Publisher’s Note: MDPI stays neutral with regard to jurisdictional claims in published maps and institutional affiliations. Results showed that increasing cellulose loading improved dimensional accuracy but reduced mechanical strength of laser-sintered parts. Sticking to the purpose of sustainable development of LS technology, this study continues to focus on improving part mechanical properties to fabricate laser-sintered 10%-CPLA parts more suitable for high-performance applications. Process parameter optimization is an effective method to improve part mechanical properties, but high laser-energy density may reduce dimensional accuracy. Excess laser energy causes the surrounding powder to stick to the part, which has a detrimental effect for hollow part fabrication such as topological parts and parts with tiny holes To solve this problem, thermal post-processing was proposed to improve the mechanical properties of laser-sintered parts fabricated using low laser energy. The porosity was evaluated by calculating the area percentage of voids from scanning electron microscope (SEM) images of sample fracture surfaces based on an image analysis method

Material Preparation
Full Factorial Laser-Sintering Experimentation
Laser-Energy Distribution
Thermal Post-Processing
Optimization of
The results also indicate that part porosity
Thermal
Conclusions
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