Abstract
Abstract The molecular configuration of motiol has been determined by the X-ray crystal analysis. The crystal of motiol iodoacetate, C32H52O2I, is monoclinic with two molecules in a unit cell of dimensions; a=17.37, b=6.78, c=13.04 Å and β=99.6°, the space group being P21. The crystal structure was solved by the heavy atom method. The atomic coordinates and anisotropic temperature factors were refined by block-diagonal matrix least-squares method. The structure determined is, in general, compatible with that derived chemically. The rings A and D are of a chair form, and the rings B and C are of a semi-chair. The molecule bends at the rings B and C to make a bow as a whole. All but one of the methyl groups are in axial junction.
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