Abstract
A useful synthesis has been developed of S-(1- and 2-halogenoalkyl)sugars in high yield and purity. Readily available sugar S-(O,O-dialkyl)phosphorodithioates undergo S–P bond rupture on reaction with fluoride ions to yield the corresponding sugar thiolates, which further react in situ with dichloromethane or 1,2-dihalogenoalkanes in the reaction medium. In this reaction, the halogenoalkanes play the role of both reactants and solvents.
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