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Abstract
The NMR spectrum of POF 3 in the nematic phase of EBBA has been measured at various temperatures. If the spectral data are interpreted in terms of a relative geometry, a deviation from the electron diffraction structure of 3° in the FPF angle is found. This discrepancy can be lifted by either assuming that the molecule distorts slightly on orientation, or by invoking large anisotropies in the indirect couplings. Quantitative estimates for both possibilities are given.
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