Abstract
An investigation of the equilibria formed between the terminal olefins 1-hexene and 1-octene and Na 2Pd 2Cl 6 in glacial acetic acid, using preparative, Raman, and ultra-violet and visible spectroscopic methods has shown that the principal olefin complexes formed are Na[Pd 2Cl 5(Olefin)], at low olefin concentrations, and [Pd 2Cl 4(Olefin) 2], at high olefin concentrations. The value is emphasised of using the Method of Continuous Variations (Job's Method) at as wide a range of wavelengths as possible for studying systems in which more than one metal—ligand complex is formed.
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