Abstract
Abstract Quantitative ir spectroscopic studies showed that the reduction of K3PMo12O40 with H2 in the early stage proceeded by consuming two bridging oxygens per Keggin anion. The process was accompanied by the stoichiometric formation of Mo5+ according to the XPS measurements. It was suggested that terminal oxygens were removed after two oxygens per Keggin anion were taken off.
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