Abstract
An indirect two-stage method for the electrosynthesis of NH2Cl was elaborated. In the first stage, NH4Cl was electrolyzed in a nondivided cell in the NaCl (aqueous solution)—CCl4 heterophase system to give NCl3 as a solution in CCl4. Under the optimum conditions, the yield of NCl3 was 80%, and the current efficiency 60%. In the second stage, the obtained solution reacted with an aqueous solution of NH3 to give an aqueous solution of NH2Cl in 50% yield (converted to NH3).
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