Abstract
Reaction of two equivalents of 5-iodo-3,4-dialkylpyrrole, in situ-generated from the corresponding tertiary butyl ester, with 5,5′-diformyldipyrromethane afforded corrole macrocycle in 20% yield. Utilization of readily available tertiary butyl 5-iodo-3,4-dialkylpyrrole-2-carboxylate and 5,5′-diformyldipyrromethane opens a simple route to corrole.
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