Abstract
Abstractexo/endo‐Hydroxylated cyclohexenones are essential synthetic intermediates for a variety of biologically active compounds. However, methods that lead to efficient and selective preparation of exo/endo‐hydroxylated cyclohexenones remain to be established. Herein, we report the practical and scalable synthesis of exo/endo‐hydroxylated cyclohexenones from readily available 2,6‐diketosulfoxides. We demonstrate that endo and exo geometric isomers of hydroxylated cyclohexenones can be obtained by simple modification of the reaction conditions.
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