Abstract
Abstractl‐[3‐13C]Alanine was synthesized from [13C]methyl iodide by using Dellaria's oxazinone, prepared from phenyl[2‐13C]bromoacetate and (S)‐2‐phenylglycinol, as a chiral glycine equivalent. Alkylation of the oxazinone with [13C]methyl iodide was achieved with high diastereoselectivity. Hydrolysis and removal of the chiral auxiliary of the alkylated oxazinone gave l‐[3‐13C]alanine. Copyright © 2003 John Wiley & Sons, Ltd.
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