Abstract

The use of ammonium hexanitratocerate(IV) in oxidimetry has been very little studied, although the salt can be obtained in a high degree of purity. Conditions have now been established for the titration of oxalic and mandelic acids with this reagent at room temperature in a nitric or hydrochloric acid medium using ferroïn as indicator. The procedures developed give precise results and they constitute definite improvements over those involving cerium IV sulphate.

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