Abstract
The combination of a bimetallic aluminium(salen) complex and tetrabutylammonium bromide was found to catalyse the synthesis of cyclic di- and trithiocarbonates from epoxides and carbon disulfide. Reactions carried out at 50 ˚C produced 1,3-oxathiolane-2-thiones, whilst at 90 ˚C, 1,3-dithiolane-2-thiones were formed.
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