Alumina and glass-bead blasting effect on bond strength of zirconia using 10-methacryloyloxydecyl dihydrogen phosphate (MDP) containing self-adhesive resin cement and primers

Abstract

In fact, bonding of zirconia restorations is still a big challenge in clinical situations and many bonding protocols discussed in literature might be still controversial. The aim of this was to study assess the bond strength of zirconia after alumina and glass-bead pre-treatments with two different primers in combination with conventional resin cement and 10-methacryloyloxydecyl dihydrogen phosphate (MDP) containing self-adhesive resin cement without priming. Fully sintered high translucent zirconia samples (n = 160) were assigned into 2 groups of pre-treatments (n = 80): Alumina-sandblasting (AB) and Glass-bead (GB). Then, each group was divided into 4 sub-groups according to priming and cement used (n = 20 each): conventional self-adhesive resin cement, MDP-silane Primer, MDP primer both with conventional self-adhesive resin cement, and MDP contained cement. Shear bond strength (SBS) was measured after thermocycling. Failure mode was analyzed using stereomicroscope. Contact angle and surface topography were investigated using other fully sintered samples (n = 30) constructed for that sole purpose, divided into control (no pre-treatment [unmodified], alumina-, and glass-bead sandblasted groups). Two-way ANOVA was performed for SBS and failure mode was analyzed. The use of Alumina-sandblasting showed higher SBS compared to Glass-bead pre-treatment for MDP-silane primer (p = 0.034) and MDP primer (p < 0.001). While MDP contained cement showed higher but insignificant SBS when pre-treated with glass-beads. Alumina-sandblasting and glass-bead pre-treatments improve bond strength of zirconia combined using primers before cementation with conventional resin cement. Also, self-adhesive MDP contained cement along with surface pre-treatment showed the highest achievable bond strength. It was concluded that both alumina-sandblasting and glass-bead blasting improved SBS combined with MDP containing self-adhesive resin cement reducing the required clinical steps during cementation of zirconia restorations.