Abstract
A much simpler and more straightforward method, alcohol interchange for the synthesis of titanium glycolate has been suggested. The method implied the reaction of tetraethyl orthosilicate with ethylene glycol on heating in air. The thermal property of titanium glycolate was characterized by thermal gravimetric (TG) and Differencial Thermal Analysis (DTA) analysis. X-ray diffraction (XRD) was used to confirm the conversion of crystalline phase of titanium glycolate from anatase to rutile. The characterization of titanium glycolate and products of its pyrolysis was conducted using scanning electron microscopes.
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