Advanced technology for in-line continuous heat soak test of tempered sheet glass to guarantee high reliability

Abstract

Advanced heat soak test (HST) technology, the ‘in-line continuous HST’ has been reported on the basis of experimental investigations and the T-T-T (time–temperature–transformation) relationship. The new HST technology is continuously carried out just after tempering (and heat strengthening) process. It was registered in ISO-20657 (2017). High temperature microscopy observations, high temperature x-ray diffractometry, differential thermal analysis, and micro-Raman spectrometry have been carried out in order to elucidate the α–β phase transformation of nickel sulphide in detail. The breakage ratio of in-line continuous HST is the same as that of conventional off-line HST or excellent. The ‘in-line continuous HST’ is already operating in a Japanese glass plant in order to produce tempered (and heat strengthened) sheet glass with high safety and reliability. The in-line continuous HST technology has the following benefits: (a) improvements of both productivity and reliability, (b) automatic inspection just after the tempering–quenching process, and (c) improvements to productive performance (many kinds products, heteromorphic products, and mass production). In this technical report, the advanced ‘in-line continuous HST’ technology which was standardised by several experimental investigations and analytical results will be shown in detail. The effective and efficient manufacturing technology of the tempered (and heat strengthened) sheet glass will be introduced.