Abstract
AbstractThe HH (35 mass% hydroxylamine hydrochloride/water solution) and HH‐ind (stabilized 35 mass% hydroxylamine hydrochloride/water solution for industrial use) decomposition reaction has an onset temperature of ∼145°C. The measured gas phase decomposition products are 0.25 mol N2 and 0.06 mol O2 per mol of hydroxylamine hydrochloride with small quantities of N2O and H2, and a trace amount of NO for a total noncondensable gas production of ∼0.39 mol/mol of hydroxylamine hydrochloride. The reaction system is tempered by the evaporation of the solvent (water) and the reaction is drastically catalyzed by stainless and carbon steel.
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