Abstract
Abstract A high performance liquid chromatographic method has been developed for the determination of active 4-tert-butyl-catechol (TBC) In 1,3-butadiene. Following evaporation of the butadiene from an aqueous m-nitrophenol internal standard solution, a 20-microliter aliquot is injected onto a reversed-phase liquid chromatographic column. Recovery op TBC was found to be quantitative over a 17-242 ppm range with a relative standard deviation of 3.8%.
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