Abstract
The dimethylsulfoxide (dmso) solvate of Th(IV) perchlorate is readily obtained from acidic aqueous Th(IV) solutions and has a formulation established from a single crystal structure determination of [Th(dmso- O) 9](ClO 4) 4 · 4dmso; triclinic, P 1 ̄ , a=12.4811(8) Å, b=12.4879(8) Å, c=23.969(2) Å, α=94.684(1)°, β=95.823(1)°, γ=119.347(1)°. The primary coordination sphere of the Th is of tricapped trigonal prismatic form, with the symmetry of the [Th(dmso- O) 9] entity being close to C 3h.
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