Abstract
A novel method for the synthesis of CL-20 by nitration of TAIW was investigated. HNO3 electrolyte, containing generated dinitrogen pentoxide and unreacted dinitrogen tetraoxide, was directly used as a nitrating agent and the result was encouraging. A series of SO3H-functionalized ionic liquids were utilized to further improve the result. The satisfactory yield of CL-20 (94%) makes it a useful method for the green and clean synthesis of CL-20.
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