Abstract

Acid-catalysed dibutyiidenation of 1-deoxy- D-glucitol and 3- O-methyl- D-glucitol yields the 2,4:5,6-diacetals as the main, thermodynamically controlled products, and 2-deoxy- D- arabino-hexitol ( i.e., 2-deoxy- D-glucitol) yields the 1,3:4,6-diacetal as the main, thermodynamically controlled product.

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