Abstract

Dental microwear analysis is an oft-used paleodietary estimation method, and the impression molds or resin casts are often analyzed rather than the original tooth surfaces. A choice of silicone products for dental impressions is crucial because the quality of microwear data is affected by the impression accuracy of the molds. For this reason, microwear researchers have heavily depended on a few commercial products such as “President” (Coltène/Whaledent AG, Switzerland) to avoid analytical errors caused using different silicone materials. Considering that the production business might be terminated, however, heavy reliance on specific products could be a potential weakness in the field. In this study, we aimed at identifying specific indexes of physical properties of silicone materials with satisfactory accuracy. For this purpose, we measured dynamic viscoelasticity and shrinkage rates of various silicone compounds, including the standard impression material President and other eight affordable dental silicones. We scanned both original tooth surface and dental impression molds with a confocal laser microscope and conducted dental microwear texture analysis (DMTA) to quantitatively compare the scanned surfaces. The results showed relationships between the material properties of silicones and impression accuracy, indicating that the materials that cured slowly and began to shrink relatively early in the hardening process were less accurate. Some of these dental impression molds showed blurred surfaces, implying that molds were peeled off from the tooth surface at the microscopic level, as the shrinkage speed might exceed the curing speed. The following indices provided in the product information were found to be helpful in the search for substitutes: (1) medium viscosity, (2) short curing time after mixing (5–6 min), and (3) delayed change in shrinkage.

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