Abstract
Comprehensive SummaryA new electrophilic monofluoromethylthiolating reagent N‐fluoromethylthiophthalimide PhthSCH2F 1 was developed. Reagent 1 could be readily synthesized from easily available starting materials benzyl mercaptan and CH2FCl in three steps. N‐Fluoromethylthiophthalimide 1 is a powerful electrophilic monofluoromethylthiolating reagent that allows the monofluoromethylthiolation of a wide range of nucleophiles including alkynes, aryl/vinyl boronic acids, electron‐rich heteroarenes, β‐ketoesters and oxindoles, as well as thiols under mild conditions.
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