Abstract
Heating of a 9-anthryldiphosphene kinetically stabilized by 2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl substituent (denoted as Bbt) group, BbtP ═ P(9-Anth) (9-Anth = 9-anthryl), with (n-Bu)3P═Te afforded 1,2-bis(9-Anth)-3-Bbt-triphosphirane in moderate yield. The structural parameters and physical properties of the isolated triphosphirane were determined by spectroscopic and X-ray crystallographic analyses.
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