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Abstract
In the cluster cation of the title compound, [Mo3S7(Et2NCS2)3](Et2NCS2), three Mo atoms form an approximately equilateral triangle, with Mo–Mo distances ranging from 2.7140 (5) to 2.7277 (5) Å, and Mo—Mo—Mo angles of ca 60°. The triangle is capped by the μ3—S atom, and each Mo—Mo bond is bridged by a disulfido group in μ2-η2 mode. Diethyldithiocarbamate ligands (Et2dtc) are chelated to the Mo atoms with an average S—Mo—S bite angle of 69.98 (1)°. There is a weak S⋯S interaction between the cluster cation and the anion (Et2dtc−).
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