Abstract
Abstract A total synthesis of the 6″-epimer of validamycin A and its diastereomer has been accomplished by a coupling reaction of the racemic peracyl 5,6-dihydroxy-1-hydroxymethyl-1,3-cyclohexadiene monoepoxide, the precursor of the unsaturated branched-chain cyclitol portion, with the protected β-d-glucopyranosylvalidamine, followed by acid hydrolysis and O-deacylation.
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