Abstract
A method for the synthesis of stereospecifically, equatorially labelled cis-M(CO) 4( 13CO)(amine) derivatives where M = Cr, Mo, and W has been developed involves 13CO substitution into the vacant coordination site created by the facile dissociation of an amine ligand from cis-M(CO) 4(amine) 2 derivatives. The mechanistic implications of this extremely stereoselective reaction are discussed.
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