Abstract
Abstract Nanocrystalline CrN was synthesized via thermal reduction–nitridation route by the reaction of CrCl3 with NH4Cl and Na in an autoclave at 400 °C. X-ray powder diffraction pattern indicated that the product was cubic CrN. An atomic ratio of Cr to N of 1.08:1 was determined from X-ray photoelectron spectra. Transmission electron microscopy image showed that the sample consisted of particles with the diameters of 20–40 nm.
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