Abstract
AbstractThe HfIV‐oxothiocluster, [Hf4(η2‐μ2‐SAc)4(η2‐μ2‐SAc)2(η2‐μ2‐BuO)4(η2‐BuO)2(μ3‐O)2], was synthesized by reaction of hafnium butoxide with thioacetic acid. The crystal structure shows the presence of a planar tetranuclear Hf4 core, in which the metal atoms are μ3‐O bridged and the thioacetate ligands coordinate the Hf ions both through a bridging and a chelating mode. The structural findings are confirmed by multinuclear NMR spectroscopic data.
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