Abstract
Al 75Mo 25 alloys were synthesized by ball milling of pure elements. The decrease of fcc aluminium peaks from the neutron diffraction patterns as a function of mechanical treatment time suggests the formation of an extended Mo(Al) solid solution, even though no significant change of the bcc lattice parameter is observed. Further evidence of the existence of a metastable phase is supplied a posteriori by in situ annealing of the processed metal powders at temperatures below 750 °C. The main product is the intermetallic Al 8Mo 3 compound.
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