Abstract
Different chiral spiroketal skeletons are obtained, in a versatile manner, by iterative alkylations of acetone N, N-dimethylhydrazone with iodides 2 followed by a one-pot deprotection/spirocyclization sequence. This methodology has been applied successfully to the synthesis of 1,7-dioxaspiro[5.5]undecane and 1,6-dioxaspiro[4.5]decane systems.
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