Abstract
A low-temperature all-solid-state thermal method has been developed to synthesize electrolytes like LiAsF6, LiPF6 and allied lithium-based fluoro-chemicals useful for lithium secondary cells. This developed procedure is simple and environmentally friendly compared with the existing procedures, which are poisonous and hazardous to health due to the use of obnoxious gases or liquids like F2, AsF3, PF3, BF3, AsF3, or AsF5, which are difficult to handle. In this proposed procedure, all chemicals are taken as analytical grade. Lithium salts and all other required salts are mixed well in required proportions and heated in between 300–400 °C to get the products examined by X-ray.
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