Abstract
AbstractA new mixed‐ligand complex, [CdL(bipy)(CH3OH)(NO3)]n (1), (HL = 4‐amino‐1‐naphthalene sulfonic acid and bipy = 4,4′‐bipyridine) could be achieved by combining d10 Cd2+ to HL and bridging ligand 4,4′‐bipy. The structure is characterized by X‐ray single‐crystal diffraction. 4‐amino‐1‐naphthalene sulfonate and 4,4′‐bipyridine act as bridging ligands, linking two adjacent CdII atom to form a two‐dimensional coordination polymer, respectively. N‐H···O hydrogen‐bonding interaction between these networks to form the face‐to‐face three‐dimensional architecture. By carrying out the reaction of polymeric cadmium naphthalene sulfonate with Na2S in the presence of sodium hydroxide, scalelike CdS materials have been obtained. The structure has been characterized by scanning electron microscopy and powder X‐ray diffraction.
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