A novel polyoxo(thio)molybdenum(V) sulfite compound: Synthesis and crystal structure of {[Mo2V(μ-S)2O2]6(μ3-SO3)4(μ-SO3)12}20−anion

Haralampos N Miras,Themistoklis A Kabanos,Alexandra M Slawin,J Derek Woollins,Peter Baran,Raphael Raptis

doi:10.1039/b309473c

A novel polyoxo(thio)molybdenum(V) sulfite compound: Synthesis and crystal structure of {[Mo2V(μ-S)2O2]6(μ3-SO3)4(μ-SO3)12}20−anion

Haralampos N Miras, Themistoklis A Kabanos + Show 4 more

https://doi.org/10.1039/b309473c

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Journal: Dalton Trans.	Publication Date: Jan 1, 2003
Citations: 21

Affiliation: University of Ioannina, University of St Andrews, University of Puerto Rico at Río Piedras

#X-ray Structure Analysis #Polyoxo Molybdate + Show 5 more

Abstract
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Abstract

The non-cyclic polyoxo(thio)molybdate(V)-sulfite K6(NH4)14{[Mo2V(μ-S)2O2]6(μ3-SO3)4(μ-SO3)12}·7H2O 1 was prepared by self-condensation of [Mo2V(μ-S)2O2]2+ building block in the presence of (NH4)2SO3. Compound 1 was characterized by X-ray structure analysis as well as IR, UV-vis spectroscopies and thermogravimetric analysis.

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