Abstract

Anions of aliphatic nitro compounds R1R2C=NO2− react with nitroso compounds RNO to give nitrones R1R2C=N(O)R. Salts of nitro compounds with metals and Et3N, as well as trimethylsilyl nitronates in the presence of F−, can serve as the sources of the anions. The structure of the nitrones was established by NMR spectroscopy. 1,3-Dipolar cycloaddition of a series of the nitrones obtained to olefins was investigated.

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