Abstract
The core–shell TiO2nano-layer spheres were synthesized by hydrothermal method without surfactant, using tetraisopropyl titanate, diethylenetriamine and water as the capping agents. The structure of the products was characterized with X-ray diffraction (XRD), transmission electron microscope (TEM) and scanning electron microscopy (SEM). The possible formation mechanism and electrocatalytic degradation characters of the products were also discussed.
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