Abstract
The single crystal structure determination of a new phase, belonging to the La-Li-Fe-O system, is reported (1456 measured reflections, R w = 0.020, space group P4 mbm ). This phase has the formula per unit cell La 24Fe 6Li 22O 56 with iron in its trivalent state. The preparative route is described, together with some equilibrium relationships with other phases, occurring in the same ternary system. The powder diffraction intensities, hkl and d ( hkl) , are also reported.
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