Abstract
AbstractThe free iodine in Wijs solution is titrated directly, in strong hydrochloric acid solution, with standard potassium iodate solution. From this titration and the usual sodium thiosulfate titration for total halogen, the iodine/chlorine ratio is calculated. Results agree closely with those obtained by the longer chlorine‐water method of Lopes. The halogen ratio of reagent grade iodine monochloride, a convenient material from which to prepare Wijs reagent directly, is also determined by the new titration method.
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