Abstract
A new cubic perovskite compound BaLaMgMnO 6− x has been prepared under high temperature (900°C) and high oxygen pressure (60–70 kbar) using in situ thermal decomposition of KClO 3 in a belt apparatus. X-Ray diffraction (XRD), redox titration, thermogravimetric analysis (TGA), and X-ray photoelectron (XPE) spectroscopy investigation have shown that x is close to 0.21 under these synthetic conditions. Mn(V) in octahedral coordination could be postulated.
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