Abstract
A new method has been proposed for the synthesis of transition metal complexes with the trans-[B20H18]2– dianion from complexes with the closo-decaborate anion [B10H10]2– without changing the cationic part of the complex. A cerium(IV) salt has been used as an oxidizing agent. Complexes [NiL3][trans-B20H18] (L = Bipy, Phen) have been identified by elemental analysis and IR spectroscopy.
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