Abstract
A dimeric Pd(III)Pd(II) complex with TCNQ was prepared in an aqueous basic solution of pH∼9. This compound was characterized by elemental analyses and spectroscopic methods - IR. UV-Vis, EPR, magnetochemistry and ESCA. The results indicate that the formula of this complex is Pd2(TCNQ)3(OH)2, (TCNQ = 7,7,8,8-tetracyano-p-quinodimethane). The ligand TCNQ may exist in two different modes - as radical-anion TCNQ· and neutral molecule TCNQ.
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