Abstract
A modified method for the production and purification of 36ClO 3 − in high yield is described. This procedure, involving the electrolytic oxidation of 36Cl − in a cell with simple electrode design and purification of the electrolysis products ( 36Cl −, 36ClO 3 −, and 36ClO 4 −) by aqueous column chromatography, allows for the recovery of about 80% of the initial radiolabel as 36ClO 3 −. The method is rapid and suitable for the production of this radiolabeled anion for use as a tracer analog for nitrate in plant membrane transport experiments.
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