Abstract

The analytical method described here will allow the preparation of corn plant tissue, the extraction of 4-aminopyridine from it, purification of the residues, and identification and estimation of the purified residue by thin-layer and gas-liquid chromatography using two dissimilar columns and two detection means — electron capture and microcoulometric nitrogen detectors. The method is sensitive to levels of 4-aminopyridine as low as 0.01 ppm.

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