Abstract
A triad of complementary techniques, namely high-resolution gas adsorption coupled with hysteresis scanning and density functional theory, rotation electron diffraction, and electron tomography, has revealed the intracrystalline nature and connectivity of size-tailored mesopores in surfactant-templated mesostructured zeolite-Y with new clarity. This approach constitutes a significant advance in the elucidation of the structure of nanoporous solids.
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