Abstract
Modern catalysis research strongly focusses on optimizing multiple reaction parameters en route to find optimal conditions. However, a very limited number of fundamental parameter combinations, such as inert conditions, gaseous reactants, variable temperature, and elevated pressure, can be screened in a convenient and straightforward manner. We report a ready-to-use reaction setup that is designed for screening reactions with gaseous reactants under inert conditions in standard NMR tubes (0.5 mL) using temperatures between −40 and +100 °C and extreme pressures. Proof-of-concept reaction examples are discussed, and the coupling to modern analytic techniques including in situ IR spectroscopy is possible.
Published Version
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