Abstract
Four O-perbenzylated glycosyl cyanides (α- and β-d-mannopyranosyl, α-d-galactopyranosyl, and α-d-arabinofuranosyl) were converted by treatment with BrCH2CO2Et/Zn in THF at reflux (Blaise-Kishi reaction) into the corresponding C-glycosyl β-enamino esters which in turn were reduced by NaBH(OAc)3 to give four pairs of C-glycosyl (R)- and (S)-β-amino esters.
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