Abstract
Abstract Treatment of diethylthioacetals with two equivalents of trityl methyl ether in the presence of a catalytic amount of trityl perchlorate, and successive quenching with aqueous sodium hydrogencarbonate gave parent carbonyl compounds, hydrolyzed products, in high yields under mild conditions. According to this method, it is also possible to hydrolyze diethylthioacetals selectively even when another thioacetal, such as 1,3-dithiane, coexisted in the same molecule.
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